Crystallography Open Database

Information card for entry 1504201

Preview

Coordinates	1504201.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28.5 H31 Cl
Calculated formula	C28.5 H31 Cl
Title of publication	A versatile preparation of Geländer-type p-terphenyls from a readily available diacetylenic precursor.
Authors of publication	Modjewski, Matthew; Lindeman, Sergey V.; Rathore, Rajendra
Journal of publication	Organic letters
Year of publication	2009
Journal volume	11
Journal issue	20
Pages of publication	4656 - 4659
a	25.9973 ± 0.0004 Å
b	12.3802 ± 0.0002 Å
c	13.8796 ± 0.0002 Å
α	90°
β	93.724 ± 0.001°
γ	90°
Cell volume	4457.74 ± 0.12 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	3
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0427
Residual factor for significantly intense reflections	0.0397
Weighted residual factors for significantly intense reflections	0.1076
Weighted residual factors for all reflections included in the refinement	0.1101
Goodness-of-fit parameter for all reflections included in the refinement	1.013
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/1504201.html