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Information card for entry 1504510
Preview
Coordinates | 1504510.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C32 H36 N O2 P |
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Calculated formula | C32 H36 N O2 P |
SMILES | P(=O)(N([C@@H](c1ccccc1)[C@H](O)C(C)(C)C)[C@@H](C)c1ccccc1)(c1ccccc1)c1ccccc1 |
Title of publication | Phosphinamide-directed benzylic lithiation. Application to the synthesis of peptide building blocks. |
Authors of publication | Burgos, Pascual Oña; Fernández, Ignacio; Iglesias, María José; García-Granda, Santiago; Ortiz, Fernando López |
Journal of publication | Organic letters |
Year of publication | 2008 |
Journal volume | 10 |
Journal issue | 4 |
Pages of publication | 537 - 540 |
a | 18.6667 ± 0.0001 Å |
b | 8.2209 ± 0.0001 Å |
c | 18.7079 ± 0.0001 Å |
α | 90° |
β | 104.9 ± 0.0006° |
γ | 90° |
Cell volume | 2774.33 ± 0.04 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 5 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0355 |
Residual factor for significantly intense reflections | 0.0309 |
Weighted residual factors for significantly intense reflections | 0.078 |
Weighted residual factors for all reflections included in the refinement | 0.0836 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.042 |
Diffraction radiation wavelength | 1.5418 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/1504510.html
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Users of the data should acknowledge the original authors of the
structural data.