Information card for entry 1505247

Structure parameters

• Formula: C17 H33 N O4 Si
• Calculated formula: C17 H33 N O4 Si
• SMILES: N1(O[C@H]2C[C@H]3OC(O[C@@H]3[C@H](O[Si](C)(C)C(C)(C)C)[C@@H]1C2)(C)C)C
• Title of publication: trans-acetonide controlled endo-selective intramolecular nitrone-alkene cycloaddition of hept-6-enoses: a facile entry to calystegines, tropanes, and hydroxylated aminocycloheptanes.
• Authors of publication: Shing, Tony K. M.; Wong, Wai F.; Ikeno, Taketo; Yamada, Tohru
• Journal of publication: Organic letters
• Year of publication: 2007
• Journal volume: 9
• Journal issue: 2
• Pages of publication: 207 - 209
• a: 8.3847 ± 0.0017 Å
• b: 10.637 ± 0.002 Å
• c: 22.556 ± 0.005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2011.7 ± 0.7 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.2339
• Residual factor for significantly intense reflections: 0.0666
• Weighted residual factors for significantly intense reflections: 0.1517
• Weighted residual factors for all reflections included in the refinement: 0.2074
• Goodness-of-fit parameter for all reflections included in the refinement: 0.941
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No