Information card for entry 1505330

Structure parameters

• Formula: C24 H29 K O6 Si
• Calculated formula: C24 H29 K O6 Si
• Title of publication: Preparation of 2-trialkylsiloxy- substituted 1,3-dienes and their diels-alder/cross-coupling reactions.
• Authors of publication: Pidaparthi, Ramakrishna R.; Welker, Mark E.; Day, Cynthia S.; Wright, Marcus W.
• Journal of publication: Organic letters
• Year of publication: 2007
• Journal volume: 9
• Journal issue: 9
• Pages of publication: 1623 - 1626
• a: 12.445 ± 0.002 Å
• b: 15.623 ± 0.003 Å
• c: 13.259 ± 0.002 Å
• α: 90°
• β: 108.108 ± 0.003°
• γ: 90°
• Cell volume: 2450.2 ± 0.7 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1187
• Residual factor for significantly intense reflections: 0.0709
• Weighted residual factors for significantly intense reflections: 0.1337
• Weighted residual factors for all reflections included in the refinement: 0.1525
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No