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Information card for entry 1505536
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Coordinates | 1505536.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C20 H17 Cl O3 |
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Calculated formula | C20.07 H16 Cl O3 |
Title of publication | Lewis acid mediated reactions of 1-cyclopropyl-2-arylethanones with allenic esters: a facile synthetic protocol for the preparation of dihydrofuro[2,3-h]chromen-2-one derivatives. |
Authors of publication | Shi, Min; Tang, Xiang-Ying; Yang, Yong-Hua |
Journal of publication | Organic letters |
Year of publication | 2007 |
Journal volume | 9 |
Journal issue | 20 |
Pages of publication | 4017 - 4020 |
a | 6.8783 ± 0.0012 Å |
b | 10.2073 ± 0.0018 Å |
c | 12.061 ± 0.002 Å |
α | 74.717 ± 0.003° |
β | 80.936 ± 0.004° |
γ | 82.909 ± 0.003° |
Cell volume | 803.7 ± 0.2 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1176 |
Residual factor for significantly intense reflections | 0.0855 |
Weighted residual factors for significantly intense reflections | 0.2556 |
Weighted residual factors for all reflections included in the refinement | 0.2846 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.007 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/1505536.html
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structural data.