Information card for entry 1506186

Structure parameters

• Formula: C26 H29 N O5
• Calculated formula: C26 H29 N O5
• Title of publication: Extending Pummerer reaction chemistry. Asymmetric synthesis of spirocyclic oxindoles via chiral indole-2-sulfoxides.
• Authors of publication: Feldman, Ken S.; Karatjas, Andrew G.
• Journal of publication: Organic letters
• Year of publication: 2006
• Journal volume: 8
• Journal issue: 18
• Pages of publication: 4137 - 4140
• a: 12.794 ± 0.003 Å
• b: 12.794 ± 0.003 Å
• c: 24.424 ± 0.007 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 3462.3 ± 1.5 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 4
• Space group number: 154
• Hermann-Mauguin space group symbol: P 32 2 1
• Hall space group symbol: P 32 2"
• Residual factor for all reflections: 0.059
• Residual factor for significantly intense reflections: 0.0562
• Weighted residual factors for significantly intense reflections: 0.1574
• Weighted residual factors for all reflections included in the refinement: 0.1626
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No