Information card for entry 1506226

Structure parameters

• Formula: C24 H32 O4
• Calculated formula: C24 H32 O4
• SMILES: O=C(O[C@H]1[C@@H](CC[C@H](C1)C)C(C)(C)c1ccccc1)[C@@H](O)c1oc(c(c1)C)C
• Title of publication: Highly diastereoselective Friedel-Crafts reaction of furans with 8-phenylmenthyl glyoxylate.
• Authors of publication: Kwiatkowski, Piotr; Majer, Jakub; Chaładaj, Wojciech; Jurczak, Janusz
• Journal of publication: Organic letters
• Year of publication: 2006
• Journal volume: 8
• Journal issue: 22
• Pages of publication: 5045 - 5048
• a: 6.0231 ± 0.0012 Å
• b: 18.81 ± 0.004 Å
• c: 19.088 ± 0.004 Å
• α: 90°
• β: 91.44 ± 0.03°
• γ: 90°
• Cell volume: 2161.9 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 3
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0968
• Residual factor for significantly intense reflections: 0.0811
• Weighted residual factors for significantly intense reflections: 0.2129
• Weighted residual factors for all reflections included in the refinement: 0.2279
• Goodness-of-fit parameter for all reflections included in the refinement: 0.993
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No