Information card for entry 1506238

Structure parameters

• Common name: 06036b
• Formula: C15 H27 N O6 Si
• Calculated formula: C15 H27 N O6 Si
• Title of publication: Silylative Dieckmann-like cyclizations of ester-imides (and diesters).
• Authors of publication: Hoye, Thomas R.; Dvornikovs, Vadims; Sizova, Elena
• Journal of publication: Organic letters
• Year of publication: 2006
• Journal volume: 8
• Journal issue: 23
• Pages of publication: 5191 - 5194
• a: 7.7751 ± 0.0017 Å
• b: 15.225 ± 0.003 Å
• c: 32.622 ± 0.007 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3861.7 ± 1.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0905
• Residual factor for significantly intense reflections: 0.0532
• Weighted residual factors for significantly intense reflections: 0.1128
• Weighted residual factors for all reflections included in the refinement: 0.1308
• Goodness-of-fit parameter for all reflections included in the refinement: 1.056
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No