Information card for entry 1506315

Structure parameters

• Common name: Hydrazine Derivative
• Chemical name: (E)-N-phthalyl-2-(3-chlorophenyl)-2-phenylcyclobutylidene hydrazine
• Formula: C24 H17 Cl N2 O2
• Calculated formula: C24 H17 Cl N2 O2
• SMILES: Clc1cccc(C2(C(=NN3C(=O)c4ccccc4C3=O)CC2)c2ccccc2)c1
• Title of publication: Nitrene equivalent mediated metal-free ring expansions of alkylidenecyclopropanes and an alkylidenecyclobutane.
• Authors of publication: Liang, Yong; Jiao, Lei; Wang, Yuanyuan; Chen, Yuanyuan; Ma, Linge; Xu, Jiaxi; Zhang, Shiwei; Yu, Zhi-Xiang
• Journal of publication: Organic letters
• Year of publication: 2006
• Journal volume: 8
• Journal issue: 25
• Pages of publication: 5877 - 5879
• a: 8.7336 ± 0.0017 Å
• b: 7.8955 ± 0.0016 Å
• c: 14.484 ± 0.003 Å
• α: 90°
• β: 95.04 ± 0.03°
• γ: 90°
• Cell volume: 994.9 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Ambient diffracton pressure: 101 kPa
• Number of distinct elements: 5
• Space group number: 7
• Hermann-Mauguin space group symbol: P 1 c 1
• Hall space group symbol: P -2yc
• Residual factor for all reflections: 0.05
• Residual factor for significantly intense reflections: 0.0393
• Weighted residual factors for significantly intense reflections: 0.0914
• Weighted residual factors for all reflections included in the refinement: 0.0947
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No