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Information card for entry 1506725
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Coordinates | 1506725.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C23 H24 O2 Sn |
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Calculated formula | C23 H23.5 O2 Sn |
Title of publication | Mechanistic studies on the O-directed free-radical hydrostannation of disubstituted acetylenes with Ph3SnH and Et3B and on the iodination of allylically oxygenated alpha-triphenylstannylalkenes. |
Authors of publication | Dimopoulos, Paschalis; George, Jonathan; Tocher, Derek A.; Manaviazar, Soraya; Hale, Karl J. |
Journal of publication | Organic letters |
Year of publication | 2005 |
Journal volume | 7 |
Journal issue | 24 |
Pages of publication | 5377 - 5380 |
a | 36.529 ± 0.003 Å |
b | 11.7506 ± 0.0009 Å |
c | 26.095 ± 0.002 Å |
α | 90° |
β | 133.184 ± 0.002° |
γ | 90° |
Cell volume | 8167.3 ± 1.1 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 4 |
Space group number | 5 |
Hermann-Mauguin space group symbol | C 1 2 1 |
Hall space group symbol | C 2y |
Residual factor for all reflections | 0.0317 |
Residual factor for significantly intense reflections | 0.0309 |
Weighted residual factors for significantly intense reflections | 0.0735 |
Weighted residual factors for all reflections included in the refinement | 0.0741 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.093 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/1506725.html
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structural data.