Information card for entry 1506905

Structure parameters

• Formula: C35 H50 N3 O5.5 Si2
• Calculated formula: C34.75 H42.5 N3 O5.5 Si2
• Title of publication: Oxidative rearrangement of imidazoles with dimethyldioxirane.
• Authors of publication: Lovely, Carl J.; Du, Hongwang; He, Yong; Rasika Dias, H. V.
• Journal of publication: Organic letters
• Year of publication: 2004
• Journal volume: 6
• Journal issue: 5
• Pages of publication: 735 - 738
• a: 14.007 ± 0.003 Å
• b: 18.438 ± 0.004 Å
• c: 29.115 ± 0.006 Å
• α: 90°
• β: 95.24 ± 0.03°
• γ: 90°
• Cell volume: 7488 ± 3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1656
• Residual factor for significantly intense reflections: 0.0888
• Weighted residual factors for all reflections: 0.3269
• Weighted residual factors for significantly intense reflections: 0.2448
• Goodness-of-fit parameter for all reflections: 0.997
• Goodness-of-fit parameter for significantly intense reflections: 1.08
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No