Information card for entry 1507573

Structure parameters

• Formula: C24 H29 N O3 S
• Calculated formula: C24 H29 N O3 S
• Title of publication: BINAPHANE-Catalyzed Asymmetric Synthesis of trans-β-Lactams from Disubstituted Ketenes and N-Tosyl Arylimines.
• Authors of publication: Chen, Shi; Salo, Eric C.; Wheeler, Kraig A.; Kerrigan, Nessan J.
• Journal of publication: Organic letters
• Year of publication: 2012
• Journal volume: 14
• Journal issue: 7
• Pages of publication: 1784 - 1787
• a: 13.2199 ± 0.0007 Å
• b: 13.2515 ± 0.0006 Å
• c: 26.9912 ± 0.0014 Å
• α: 90°
• β: 90.321 ± 0.004°
• γ: 90°
• Cell volume: 4728.3 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0649
• Residual factor for significantly intense reflections: 0.0499
• Weighted residual factors for all reflections: 0.1232
• Weighted residual factors for significantly intense reflections: 0.1164
• Goodness-of-fit parameter for all reflections: 1.009
• Goodness-of-fit parameter for significantly intense reflections: 1.071
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No