Information card for entry 1508156

Structure parameters

• Formula: C44 H146 Dy2 N10 O92 P2 W22
• Calculated formula: C44 H126 Dy2 N10 O92 P2 W22
• Title of publication: Syntheses, structures and properties of dimeric rare earth derivatives based on monovacant Keggin-type polyoxotungstates
• Authors of publication: Zhang, Dongdi; Zhang, Chao; Chen, Huanni; Ma, Pengtao; Wang, Jingping; Niu, Jingyang
• Journal of publication: Inorganica Chimica Acta
• Year of publication: 2012
• Journal volume: 391
• Pages of publication: 218 - 223
• a: 25.113 ± 0.002 Å
• b: 12.7316 ± 0.0012 Å
• c: 22.36 ± 0.002 Å
• α: 90°
• β: 115.173 ± 0.001°
• γ: 90°
• Cell volume: 6470.2 ± 1 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0669
• Residual factor for significantly intense reflections: 0.0461
• Weighted residual factors for significantly intense reflections: 0.103
• Weighted residual factors for all reflections included in the refinement: 0.1112
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No