Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 1508699
Preview
Jmol._Canvas2D (Jmol) "jmolApplet0"[x]
Coordinates | 1508699.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C15 H23 N O3 |
---|---|
Calculated formula | C15 H23 N O3 |
Title of publication | Synthesis and reduction kinetics of sterically shielded pyrrolidine nitroxides. |
Authors of publication | Paletta, Joseph T.; Pink, Maren; Foley, Bridget; Rajca, Suchada; Rajca, Andrzej |
Journal of publication | Organic letters |
Year of publication | 2012 |
Journal volume | 14 |
Journal issue | 20 |
Pages of publication | 5322 - 5325 |
a | 8.025 ± 0.0004 Å |
b | 9.9052 ± 0.0005 Å |
c | 8.9614 ± 0.0004 Å |
α | 90° |
β | 92.41 ± 0.001° |
γ | 90° |
Cell volume | 711.7 ± 0.06 Å3 |
Cell temperature | 150 K |
Ambient diffraction temperature | 150 K |
Number of distinct elements | 4 |
Space group number | 11 |
Hermann-Mauguin space group symbol | P 1 21/m 1 |
Hall space group symbol | -P 2yb |
Residual factor for all reflections | 0.106 |
Residual factor for significantly intense reflections | 0.0963 |
Weighted residual factors for all reflections | 0.2912 |
Weighted residual factors for significantly intense reflections | 0.2519 |
Weighted residual factors for all reflections included in the refinement | 0.2618 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.0709 |
Diffraction radiation wavelength | 0.41238 Å |
Diffraction radiation type | synchrotron |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/1508699.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.