Information card for entry 1512823

Structure parameters

• Formula: C37 H48 N4 Ni2 O9 S2
• Calculated formula: C37 H36 N4 Ni2 O9 S2
• Title of publication: Polynuclear nickel(II) complexes with salicylaldimine derivative ligands
• Authors of publication: Moussa Dieng; Ousmane Diouf; Mohamed Gaye; Abdou Salam Sall; Paulo Perez-Lourido; Laura Valencia; Andrea Caneschi; Lorenzo Sorace
• Journal of publication: Inorganica Chimica Acta
• Year of publication: 2013
• Journal volume: 394
• Pages of publication: 741 - 746
• a: 13.8664 ± 0.0018 Å
• b: 14.8691 ± 0.0019 Å
• c: 21.014 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4332.7 ± 1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 60
• Hermann-Mauguin space group symbol: P b c n
• Hall space group symbol: -P 2n 2ab
• Residual factor for all reflections: 0.0906
• Residual factor for significantly intense reflections: 0.0672
• Weighted residual factors for significantly intense reflections: 0.2205
• Weighted residual factors for all reflections included in the refinement: 0.2586
• Goodness-of-fit parameter for all reflections included in the refinement: 1.1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No