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Information card for entry 1513241
Preview
Coordinates | 1513241.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C24 H44 O3 Si |
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Calculated formula | C24 H44 O3 Si |
SMILES | [Si](O[C@H]1C[C@@H]2[C@]3(CC[C@H](O)C(C)(C)[C@@H]3CC(=O)[C@H]2[C@H](C1)C)C)(C)(C)C(C)(C)C |
Title of publication | Total synthesis of (+)-cassaine utilizing an anionic polycyclization strategy. |
Authors of publication | Ravindar, Kontham; Caron, Pierre-Yves; Deslongchamps, Pierre |
Journal of publication | Organic letters |
Year of publication | 2013 |
Journal volume | 15 |
Journal issue | 24 |
Pages of publication | 6270 - 6273 |
a | 14.8863 ± 0.0002 Å |
b | 25.4284 ± 0.0004 Å |
c | 6.6202 ± 0.0001 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 2505.98 ± 0.06 Å3 |
Cell temperature | 296 ± 2 K |
Ambient diffraction temperature | 296 ± 2 K |
Number of distinct elements | 4 |
Space group number | 18 |
Hermann-Mauguin space group symbol | P 21 21 2 |
Hall space group symbol | P 2 2ab |
Residual factor for all reflections | 0.048 |
Residual factor for significantly intense reflections | 0.0444 |
Weighted residual factors for significantly intense reflections | 0.1221 |
Weighted residual factors for all reflections included in the refinement | 0.1261 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.066 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/1513241.html
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