Information card for entry 1513848

Structure parameters

• Common name: Gandelman-155 (Saha)
• Formula: C48 H64 F12 N3 O3.5 P4 Rh
• Calculated formula: C48 H64 F12 N3 O3.5 P4 Rh
• Title of publication: Cation‒cation bonding in nitrenium metal complexes
• Authors of publication: Tulchinsky, Yuri; Kozuch, Sebastian; Saha, Prasenjit; Botoshansky, Mark; Shimon, Linda J. W.; Gandelman, Mark
• Journal of publication: Chemical Science
• Year of publication: 2014
• Journal volume: 5
• Journal issue: 4
• Pages of publication: 1305
• a: 13.854 ± 0.002 Å
• b: 22.376 ± 0.003 Å
• c: 19.553 ± 0.003 Å
• α: 90°
• β: 109.609 ± 0.004°
• γ: 90°
• Cell volume: 5709.8 ± 1.4 ų
• Cell temperature: 240 ± 2 K
• Ambient diffraction temperature: 240 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1002
• Residual factor for significantly intense reflections: 0.0729
• Weighted residual factors for significantly intense reflections: 0.22
• Weighted residual factors for all reflections included in the refinement: 0.2551
• Goodness-of-fit parameter for all reflections included in the refinement: 1.075
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No