Information card for entry 1514258

Structure parameters

• Formula: C26 H28 N2 O2 Si
• Calculated formula: C26 H28 N2 O2 Si
• SMILES: [Si](C(Cc1ccc(cc1)N(=O)=O)=C=NC(c1ccccc1)(c1ccccc1)C)(C)(C)C
• Title of publication: Exploring the anionic reactivity of ynimines, useful precursors of metalated ketenimines.
• Authors of publication: Laouiti, Anouar; Couty, François; Marrot, Jérome; Boubaker, Taoufik; Rammah, Mohamed M; Rammah, Mohamed B; Evano, Gwilherm
• Journal of publication: Organic letters
• Year of publication: 2014
• Journal volume: 16
• Journal issue: 8
• Pages of publication: 2252 - 2255
• a: 19.789 ± 0.003 Å
• b: 6.2044 ± 0.0012 Å
• c: 20.095 ± 0.003 Å
• α: 90°
• β: 100.538 ± 0.008°
• γ: 90°
• Cell volume: 2425.6 ± 0.7 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1453
• Residual factor for significantly intense reflections: 0.0713
• Weighted residual factors for significantly intense reflections: 0.1841
• Weighted residual factors for all reflections included in the refinement: 0.2327
• Goodness-of-fit parameter for all reflections included in the refinement: 1.061
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No