Information card for entry 1514732

Structure parameters

• Formula: C30 H42 N2 Si
• Calculated formula: C30 H42 N2 Si
• SMILES: [SiH](Nc1c(C(C)C)cccc1C(C)C)(Nc1c(C(C)C)cccc1C(C)C)c1ccccc1
• Title of publication: Hetero-dehydrocoupling of silanes and amines by heavier alkaline earth catalysis
• Authors of publication: Hill, Michael S.; Liptrot, David J.; MacDougall, Dugald J.; Mahon, Mary F.; Robinson, Thomas P.
• Journal of publication: Chemical Science
• Year of publication: 2013
• Journal volume: 4
• Journal issue: 11
• Pages of publication: 4212
• a: 15.1354 ± 0.0004 Å
• b: 9.24 ± 0.0003 Å
• c: 20.128 ± 0.0006 Å
• α: 90°
• β: 101.781 ± 0.002°
• γ: 90°
• Cell volume: 2755.63 ± 0.14 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/a 1
• Hall space group symbol: -P 2yab
• Residual factor for all reflections: 0.0757
• Residual factor for significantly intense reflections: 0.0578
• Weighted residual factors for significantly intense reflections: 0.1372
• Weighted residual factors for all reflections included in the refinement: 0.1484
• Goodness-of-fit parameter for all reflections included in the refinement: 1.105
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No