Information card for entry 1514821

Structure parameters

• Common name: [(OAc)Ni(Medoen)Zn(Me3TACN)]ClO4
• Formula: C21 H40 Cl N7 Ni O8 Zn
• Calculated formula: C21 H37.096 Cl N7 Ni O8.1 Zn
• Title of publication: Access to formally Ni(i) states in a heterobimetallic NiZn system
• Authors of publication: Uyeda, Christopher; Peters, Jonas C.
• Journal of publication: Chemical Science
• Year of publication: 2013
• Journal volume: 4
• Journal issue: 1
• Pages of publication: 157
• a: 18.853 ± 0.004 Å
• b: 18.337 ± 0.004 Å
• c: 16.409 ± 0.003 Å
• α: 90°
• β: 90.05 ± 0.03°
• γ: 90°
• Cell volume: 5673 ± 2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0711
• Residual factor for significantly intense reflections: 0.0474
• Weighted residual factors for significantly intense reflections: 0.0998
• Weighted residual factors for all reflections included in the refinement: 0.1142
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No