Information card for entry 1514959

Structure parameters

• Formula: C54 H52 N4 O2
• Calculated formula: C54 H52 N4 O2
• Title of publication: Synthesis and oxidation of cyclic tetraindole
• Authors of publication: Nakamura, Shoichi; Hiroto, Satoru; Shinokubo, Hiroshi
• Journal of publication: Chemical Science
• Year of publication: 2012
• Journal volume: 3
• Journal issue: 2
• Pages of publication: 524
• a: 17.198 ± 0.004 Å
• b: 17.198 ± 0.004 Å
• c: 15.807 ± 0.007 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4675 ± 3 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 4
• Space group number: 120
• Hermann-Mauguin space group symbol: I -4 c 2
• Hall space group symbol: I -4 -2c
• Residual factor for all reflections: 0.1032
• Residual factor for significantly intense reflections: 0.0745
• Weighted residual factors for significantly intense reflections: 0.1881
• Weighted residual factors for all reflections included in the refinement: 0.2068
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No