Information card for entry 1515413

Structure parameters

• Formula: C47 H59 Cl3 N4 O8 Si
• Calculated formula: C47 H59 Cl3 N4 O8 Si
• Title of publication: Total synthesis of diazonamide A.
• Authors of publication: Knowles, Robert R.; Carpenter, Joseph; Blakey, Simon B.; Kayano, Akio; Mangion, Ian K.; Sinz, Christopher J.; Macmillan, David W. C.
• Journal of publication: Chemical science (Royal Society of Chemistry : 2010)
• Year of publication: 2011
• Journal volume: 2011
• Journal issue: 2
• Pages of publication: 308 - 311
• a: 19.546 ± 0.004 Å
• b: 17.36 ± 0.004 Å
• c: 19.889 ± 0.004 Å
• α: 90°
• β: 105.63 ± 0.03°
• γ: 90°
• Cell volume: 6499 ± 3 ų
• Cell temperature: 200 ± 1 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 6
• Space group number: 5
• Hermann-Mauguin space group symbol: C 1 2 1
• Hall space group symbol: C 2y
• Residual factor for all reflections: 0.1515
• Residual factor for significantly intense reflections: 0.1136
• Weighted residual factors for significantly intense reflections: 0.2908
• Weighted residual factors for all reflections included in the refinement: 0.3174
• Goodness-of-fit parameter for all reflections included in the refinement: 1.111
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No