Information card for entry 1515593

Structure parameters

• Formula: C134 H192 N10 O6 S0.02 Se0.98 U2
• Calculated formula: C134 H192 N10 O6 S0.024 Se0.976 U2
• Title of publication: Activation of elemental S, Se and Te with uranium(iii): bridging U‒E‒U (E = S, Se) and diamond-core complexes U‒(E)2‒U (E = O, S, Se, Te)
• Authors of publication: Lam, Oanh P.; Heinemann, Frank W.; Meyer, Karsten
• Journal of publication: Chemical Science
• Year of publication: 2011
• Journal volume: 2
• Journal issue: 8
• Pages of publication: 1538
• a: 14.8605 ± 0.0019 Å
• b: 15.046 ± 0.002 Å
• c: 17.8037 ± 0.0016 Å
• α: 70.931 ± 0.009°
• β: 81.732 ± 0.011°
• γ: 60.483 ± 0.01°
• Cell volume: 3273.3 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0495
• Residual factor for significantly intense reflections: 0.0387
• Weighted residual factors for significantly intense reflections: 0.092
• Weighted residual factors for all reflections included in the refinement: 0.0969
• Goodness-of-fit parameter for all reflections included in the refinement: 1.101
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No