Information card for entry 1515597

Structure parameters

• Formula: C132 H192 N2 Na2 O18 Se2 U2
• Calculated formula: C132 H192 N2 Na2 O18 Se2 U2
• Title of publication: Activation of elemental S, Se and Te with uranium(iii): bridging U‒E‒U (E = S, Se) and diamond-core complexes U‒(E)2‒U (E = O, S, Se, Te)
• Authors of publication: Lam, Oanh P.; Heinemann, Frank W.; Meyer, Karsten
• Journal of publication: Chemical Science
• Year of publication: 2011
• Journal volume: 2
• Journal issue: 8
• Pages of publication: 1538
• a: 24.887 ± 0.005 Å
• b: 21.404 ± 0.004 Å
• c: 26.847 ± 0.005 Å
• α: 90°
• β: 110.322 ± 0.009°
• γ: 90°
• Cell volume: 13411 ± 5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0897
• Residual factor for significantly intense reflections: 0.0527
• Weighted residual factors for significantly intense reflections: 0.1219
• Weighted residual factors for all reflections included in the refinement: 0.1345
• Goodness-of-fit parameter for all reflections included in the refinement: 1.082
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No