Information card for entry 1515951

Structure parameters

• Formula: C46 H66 Cl4 K2 N2 O13 Pt2
• Calculated formula: C46 H56 Cl4 K2 N2 O13 Pt2
• Title of publication: Synthesis, crystal structure, solution and spectroscopic properties, and hydrogen-evolving activity of [K(18-crown-6)][Pt(ii)(2-phenylpyridinato)Cl2]
• Authors of publication: Kobayashi, Masayuki; Masaoka, Shigeyuki; Sakai, Ken
• Journal of publication: Photochemical & Photobiological Sciences
• Year of publication: 2009
• Journal volume: 8
• Journal issue: 2
• Pages of publication: 196
• a: 10.6085 ± 0.0018 Å
• b: 14.149 ± 0.002 Å
• c: 19.981 ± 0.004 Å
• α: 110.6 ± 0.002°
• β: 103.178 ± 0.002°
• γ: 92.221 ± 0.002°
• Cell volume: 2710.1 ± 0.8 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0776
• Residual factor for significantly intense reflections: 0.0652
• Weighted residual factors for significantly intense reflections: 0.158
• Weighted residual factors for all reflections included in the refinement: 0.1632
• Goodness-of-fit parameter for all reflections included in the refinement: 1.132
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No