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Information card for entry 1516264
Preview
Coordinates | 1516264.cif |
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Original paper (by DOI) | HTML |
Formula | C24 H25 Cl N2 O4 |
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Calculated formula | C24 H25 Cl N2 O4 |
SMILES | Clc1ccc2N(C(=O)[C@]3(N(C(=O)[C@@]3(CC)c3ccccc3)C(=O)OC(C)(C)C)c2c1)C |
Title of publication | Bifunctional N-Heterocyclic Carbene-Catalyzed Highly Enantioselective Synthesis of Spirocyclic Oxindolo-β-lactams. |
Authors of publication | Zhang, Han-Ming; Gao, Zhong-Hua; Ye, Song |
Journal of publication | Organic letters |
Year of publication | 2014 |
Journal volume | 16 |
Journal issue | 11 |
Pages of publication | 3079 - 3081 |
a | 11.939 ± 0.002 Å |
b | 12.451 ± 0.003 Å |
c | 15.057 ± 0.003 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 2238.3 ± 0.8 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 5 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0406 |
Residual factor for significantly intense reflections | 0.0388 |
Weighted residual factors for significantly intense reflections | 0.0851 |
Weighted residual factors for all reflections included in the refinement | 0.0865 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.048 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/1516264.html
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