Information card for entry 1516449

Structure parameters

• Formula: C27 H38 B F4 N O0.5 P Rh
• Calculated formula: C27 H34 B F4 N O0.5 P Rh
• Title of publication: Cationic Rhodium Complexes with Hemilabile Phosphine Ligands as Polymerization Catalyst for High Molecular Weight Stereoregular Poly(phenylacetylene)
• Authors of publication: Jiménez, M. Victoria; Pérez-Torrente, Jesús J.; Bartolomé, M. Isabel; Vispe, Eugenio; Lahoz, Fernando J.; Oro, Luis A.
• Journal of publication: Macromolecules
• Year of publication: 2009
• Journal volume: 42
• Journal issue: 21
• Pages of publication: 8146
• a: 9.4341 ± 0.0006 Å
• b: 9.8954 ± 0.0006 Å
• c: 14.835 ± 0.001 Å
• α: 92.365 ± 0.001°
• β: 107.922 ± 0.001°
• γ: 95.181 ± 0.001°
• Cell volume: 1308.84 ± 0.15 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0442
• Residual factor for significantly intense reflections: 0.0392
• Weighted residual factors for significantly intense reflections: 0.0939
• Weighted residual factors for all reflections included in the refinement: 0.0968
• Goodness-of-fit parameter for all reflections included in the refinement: 1.007
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No