Crystallography Open Database

Information card for entry 1517022

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Coordinates	1517022.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C38 H42 Au P Si
Calculated formula	C38 H42 Au P Si
Title of publication	The Gilded Edge in Acetylenic Scaffolding: Pd-Catalyzed Cross-Coupling Reactions of Phosphine-Gold(I) Oligoynyl Complexes.
Authors of publication	Mazzanti, Virginia; Jiang, Huixin; Gotfredsen, Henrik; Morsing, Thorbjørn J; Parker, Christian R.; Nielsen, Mogens Brøndsted
Journal of publication	Organic letters
Year of publication	2014
Journal volume	16
Journal issue	14
Pages of publication	3736
a	25.9774 ± 0.0015 Å
b	25.2649 ± 0.0015 Å
c	11.2161 ± 0.0006 Å
α	90°
β	113.278 ± 0.002°
γ	90°
Cell volume	6762.1 ± 0.7 Å³
Cell temperature	122 ± 2 K
Ambient diffraction temperature	122 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0362
Residual factor for significantly intense reflections	0.0249
Weighted residual factors for significantly intense reflections	0.0594
Weighted residual factors for all reflections included in the refinement	0.0663
Goodness-of-fit parameter for all reflections included in the refinement	1.0753
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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