Information card for entry 1517058

Structure parameters

• Formula: C20 H22 N3 Ni O8 P2
• Calculated formula: C20 H22 N3 Ni O8 P2
• Title of publication: Hydrothermal syntheses and structural chemistry of Mn(II), Co(II) and Ni(II) coordination polymers with xylyl-diphosphonate ligands
• Authors of publication: Tiffany M. Smith; Diona Symester; Kathryn Perrin; Jose Vargas; Michael Tichenor; Charles J. O-Connor; Jon Zubieta
• Journal of publication: Inorganica Chimica Acta
• Year of publication: 2013
• Journal volume: 402
• Pages of publication: 46 - 59
• a: 10.8732 ± 0.0005 Å
• b: 11.0085 ± 0.0005 Å
• c: 11.2619 ± 0.0005 Å
• α: 63.681 ± 0.002°
• β: 66.155 ± 0.002°
• γ: 72.92 ± 0.002°
• Cell volume: 1094.32 ± 0.09 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0309
• Residual factor for significantly intense reflections: 0.0305
• Weighted residual factors for significantly intense reflections: 0.0893
• Weighted residual factors for all reflections included in the refinement: 0.0896
• Goodness-of-fit parameter for all reflections included in the refinement: 0.93
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No