Information card for entry 1517618

Structure parameters

• Formula: C19.5 H19.5 N8.5 Ni O4.5
• Calculated formula: C19.5 H19.5 N8.5 Ni O4.5
• Title of publication: Coordination polymers of transition metals derived from the in situ nucleophilic addition of alcohols to dicyanonitrosomethanide [C(CN)2(NO)]-
• Authors of publication: Mohd. R. Razali; Aron Urbatsch; Glen B. Deacon; Stuart R. Batten
• Journal of publication: Inorganica Chimica Acta
• Year of publication: 2013
• Journal volume: 403
• Pages of publication: 120 - 126
• a: 10.975 ± 0.002 Å
• b: 11.641 ± 0.002 Å
• c: 13.659 ± 0.003 Å
• α: 92.24 ± 0.03°
• β: 96.77 ± 0.03°
• γ: 115.1 ± 0.03°
• Cell volume: 1561.5 ± 0.7 ų
• Cell temperature: 123 ± 0.18 K
• Ambient diffraction temperature: 123 ± 0.18 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0758
• Residual factor for significantly intense reflections: 0.0613
• Weighted residual factors for significantly intense reflections: 0.1879
• Weighted residual factors for all reflections included in the refinement: 0.1979
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No