Information card for entry 1517859

Structure parameters

• Formula: C150 H179.5 N2 O6.35 Te2 U2
• Calculated formula: C150 H179.5 N2 O6.35 Te2 U2
• Title of publication: Reactivity of uranium(iii) with H2E (E = S, Se, Te): synthesis of a series of mononuclear and dinuclear uranium(iv) hydrochalcogenido complexes
• Authors of publication: Franke, Sebastian M.; Rosenzweig, Michael W.; Heinemann, Frank W.; Meyer, Karsten
• Journal of publication: Chem. Sci.
• Year of publication: 2015
• Journal volume: 6
• Journal issue: 1
• Pages of publication: 275
• a: 16.773 ± 0.0006 Å
• b: 16.923 ± 0.0016 Å
• c: 25.039 ± 0.003 Å
• α: 105.196 ± 0.006°
• β: 102.968 ± 0.007°
• γ: 101.507 ± 0.007°
• Cell volume: 6426.8 ± 1.1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.055
• Residual factor for significantly intense reflections: 0.036
• Weighted residual factors for significantly intense reflections: 0.075
• Weighted residual factors for all reflections included in the refinement: 0.0839
• Goodness-of-fit parameter for all reflections included in the refinement: 1.165
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No