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Information card for entry 1518262
Preview
Coordinates | 1518262.cif |
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Original paper (by DOI) | HTML |
Formula | C28 H37 N O4 S Si |
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Calculated formula | C28 H37 N O4 S Si |
SMILES | c1cc(ccc1C(=C\C#C[Si](C(C)C)(C(C)C)C(C)C)\C(=O)NS(=O)(=O)c1ccc(C)cc1)OC |
Title of publication | Rhodium(III)-catalyzed olefinic C-H alkynylation of acrylamides using tosyl-imide as directing group. |
Authors of publication | Feng, Chao; Feng, Daming; Luo, Yang; Loh, Teck-Peng |
Journal of publication | Organic letters |
Year of publication | 2014 |
Journal volume | 16 |
Journal issue | 22 |
Pages of publication | 5956 - 5959 |
a | 8.086 ± 0.0012 Å |
b | 8.8985 ± 0.0014 Å |
c | 20.084 ± 0.003 Å |
α | 89.551 ± 0.004° |
β | 83.782 ± 0.004° |
γ | 84.105 ± 0.004° |
Cell volume | 1429 ± 0.4 Å3 |
Cell temperature | 103 ± 2 K |
Ambient diffraction temperature | 103 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.159 |
Residual factor for significantly intense reflections | 0.1233 |
Weighted residual factors for significantly intense reflections | 0.3208 |
Weighted residual factors for all reflections included in the refinement | 0.3446 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.123 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/1518262.html
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