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Information card for entry 1518458
Preview
Coordinates | 1518458.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C24 H25 N O5 |
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Calculated formula | C24 H25 N O5 |
SMILES | O(C(=O)C1(C(=O)OC)[C@@H](c2c3c([nH]c2[C@H](C1)C=C)cccc3)c1ccccc1)C.O |
Title of publication | Palladium-catalyzed asymmetric cycloadditions of vinylcyclopropanes and in situ formed unsaturated imines: construction of structurally and optically enriched spiroindolenines. |
Authors of publication | Liu, Ze-Shui; Li, Wen-Ke; Kang, Tai-Ran; He, Long; Liu, Quan-Zhong |
Journal of publication | Organic letters |
Year of publication | 2015 |
Journal volume | 17 |
Journal issue | 1 |
Pages of publication | 150 - 153 |
a | 9.0419 ± 0.0001 Å |
b | 12.2803 ± 0.0002 Å |
c | 19.0748 ± 0.0002 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 2118.01 ± 0.05 Å3 |
Cell temperature | 291 ± 2 K |
Ambient diffraction temperature | 291 ± 2 K |
Number of distinct elements | 4 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0303 |
Residual factor for significantly intense reflections | 0.0298 |
Weighted residual factors for significantly intense reflections | 0.0823 |
Weighted residual factors for all reflections included in the refinement | 0.0829 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.096 |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/1518458.html
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