Information card for entry 1518639

Structure parameters

• Formula: C33 H40 B N O4 Si
• Calculated formula: C33 H40 B N O4 Si
• Title of publication: Silicon-tethered strategy for copper(i)-catalyzed stereo- and regioselective alkylboration of alkynes.
• Authors of publication: Kubota, Koji; Iwamoto, Hiroaki; Yamamoto, Eiji; Ito, Hajime
• Journal of publication: Organic letters
• Year of publication: 2015
• Journal volume: 17
• Journal issue: 3
• Pages of publication: 620 - 623
• a: 13.3949 ± 0.001 Å
• b: 14.3478 ± 0.0012 Å
• c: 15.283 ± 0.0012 Å
• α: 90°
• β: 92.281 ± 0.003°
• γ: 90°
• Cell volume: 2934.9 ± 0.4 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.097
• Weighted residual factors for all reflections included in the refinement: 0.3491
• Goodness-of-fit parameter for all reflections included in the refinement: 1.16
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No