Information card for entry 1518804

Structure parameters

• Formula: C58 H74 Mo2 N4 O5
• Calculated formula: C58 H74 Mo2 N4 O5
• Title of publication: Synthesis and structure of mixed carboxylate-aminopyridinate and -amidinate complexes of dimolybdenum and ditungsten
• Authors of publication: Irene Mendoza; Natalia Curado; Mario Carrasco; Eleuterio Alvarez; Riccardo Peloso; Amor Rodriguez; Ernesto Carmona
• Journal of publication: Inorganica Chimica Acta
• Year of publication: 2015
• Journal volume: 424
• Pages of publication: 120 - 128
• a: 11.1913 ± 0.0005 Å
• b: 12.1888 ± 0.0005 Å
• c: 12.4422 ± 0.0006 Å
• α: 89.5 ± 0.002°
• β: 66.097 ± 0.001°
• γ: 65.18 ± 0.001°
• Cell volume: 1381.45 ± 0.11 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0254
• Residual factor for significantly intense reflections: 0.0233
• Weighted residual factors for significantly intense reflections: 0.0592
• Weighted residual factors for all reflections included in the refinement: 0.0604
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No