Information card for entry 1518856

Structure parameters

• Formula: C47.53 H82 O11.52 P2 Ru2
• Calculated formula: C47.526 H78 O11.526 P2 Ru2
• Title of publication: Compromising the metal-metal bond in diruthenium(II,III) tetraacetate: Reaction of [Ru2(mu-O2CMe)4(MeOH)2]+ with phosphines to form 'Ru(mu-O2CMe)2(mu-OMe)2Ru' cores
• Authors of publication: Elizabeth G. Corkum; Ruiyao Wang; Manuel A.S. Aquino
• Journal of publication: Inorganica Chimica Acta
• Year of publication: 2015
• Journal volume: 424
• Pages of publication: 202 - 209
• a: 11.1632 ± 0.0001 Å
• b: 14.5311 ± 0.0002 Å
• c: 15.83 ± 0.0002 Å
• α: 90°
• β: 90.206 ± 0.001°
• γ: 90°
• Cell volume: 2567.82 ± 0.05 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.029
• Residual factor for significantly intense reflections: 0.0246
• Weighted residual factors for significantly intense reflections: 0.0595
• Weighted residual factors for all reflections included in the refinement: 0.0618
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No