Crystal Structures of Salts of Mono- and Triprotonated [36]Adamanzane, 1,5,9,13-Tetraazatricyclo[7.7.3.3(5,13)]docosane, and Equilibrium Studies of the Reactions between Mono-, Di- and Triprotonated Species, Respectively, Having None, One and Two Lone Pairs Pointing Outwards
Authors of publication
Springborg, Johan; Pretzmann, Ulla; Olsen, Carl Erik; Sotofte, Inger
Journal of publication
Acta Chemica Scandinavica
Year of publication
1998
Journal volume
52
Pages of publication
289 - 295
a
9.384 ± 0.003 Å
b
9.63 ± 0.003 Å
c
15.31 ± 0.003 Å
α
97.87 ± 0.03°
β
91.23 ± 0.03°
γ
97.77 ± 0.03°
Cell volume
1356.8 ± 0.7 Å3
Ambient diffraction temperature
120 K
Number of distinct elements
6
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for significantly intense reflections
0.0962
Weighted residual factors for significantly intense reflections
