Information card for entry 1520707

Structure parameters

• Formula: C20 H23 N O8
• Calculated formula: C20 H23 N O8
• Title of publication: Total Synthesis of (+)-3-Demethoxyerythratidinone and (+)-Erysotramidine via the Oxidative Amidation of a Phenol.
• Authors of publication: Paladino, Marco; Zaifman, Joshua; Ciufolini, Marco A.
• Journal of publication: Organic letters
• Year of publication: 2015
• Journal volume: 17
• Journal issue: 14
• Pages of publication: 3422 - 3425
• a: 8.7215 ± 0.0006 Å
• b: 11.3257 ± 0.0008 Å
• c: 19.217 ± 0.001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1898.2 ± 0.2 ų
• Cell temperature: 90 ± 0.1 K
• Ambient diffraction temperature: 90 ± 0.1 K
• Number of distinct elements: 4
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0277
• Residual factor for significantly intense reflections: 0.0269
• Weighted residual factors for significantly intense reflections: 0.0672
• Weighted residual factors for all reflections included in the refinement: 0.068
• Goodness-of-fit parameter for all reflections included in the refinement: 1.072
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No