Information card for entry 1520728

Structure parameters

• Common name: QY614
• Chemical name: Doyle-Quian QY614
• Formula: C25 H34 N2 O9 Si
• Calculated formula: C25 H34 N2 O9 Si
• Title of publication: Lewis Acid/Rhodium-Catalyzed Formal [3 + 3]-Cycloaddition of Enoldiazoacetates with Donor-Acceptor Cyclopropanes.
• Authors of publication: Cheng, Qing-Qing; Qian, Yu; Zavalij, Peter Y.; Doyle, Michael P.
• Journal of publication: Organic letters
• Year of publication: 2015
• Journal volume: 17
• Journal issue: 14
• Pages of publication: 3568 - 3571
• a: 10.3059 ± 0.0007 Å
• b: 20.6482 ± 0.0013 Å
• c: 25.5756 ± 0.0017 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5442.4 ± 0.6 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0387
• Residual factor for significantly intense reflections: 0.0329
• Weighted residual factors for significantly intense reflections: 0.0648
• Weighted residual factors for all reflections included in the refinement: 0.0666
• Goodness-of-fit parameter for all reflections included in the refinement: 1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No