Information card for entry 1520747

Structure parameters

• Formula: C42 H69 Al N2 Rh Si
• Calculated formula: C42 H69 Al N2 Rh Si
• Title of publication: Addition of aluminium, zinc and magnesium hydrides to rhodium(iii)
• Authors of publication: Ekkert, Olga; White, Andrew J. P.; Toms, Harold; Crimmin, Mark R.
• Journal of publication: Chem. Sci.
• Year of publication: 2015
• Journal volume: 6
• Journal issue: 10
• Pages of publication: 5617
• a: 10.8994 ± 0.0003 Å
• b: 20.7161 ± 0.0005 Å
• c: 18.9857 ± 0.0004 Å
• α: 90°
• β: 92.16 ± 0.002°
• γ: 90°
• Cell volume: 4283.79 ± 0.18 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0549
• Residual factor for significantly intense reflections: 0.0374
• Weighted residual factors for significantly intense reflections: 0.0801
• Weighted residual factors for all reflections included in the refinement: 0.0898
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No