Information card for entry 1520765

Structure parameters

• Formula: C32 H102.5 Mo8 N14 O53.25 P4
• Calculated formula: C32 H36 Mo8 N6 O61.25 P4
• Title of publication: Fully Oxidized and Mixed-Valent Polyoxomolybdates Structured by Bisphosphonates with Pendant Pyridine Groups: Synthesis, Structure and Photochromic Properties
• Authors of publication: Oms, Olivier; Benali, Tarik; Marrot, Jérome; Mialane, Pierre; Puget, Marin; Serier-Brault, Hélène; Deniard, Philippe; Dessapt, Rémi; Dolbecq, Anne
• Journal of publication: Inorganics
• Year of publication: 2015
• Journal volume: 3
• Journal issue: 2
• Pages of publication: 279
• a: 17.6023 ± 0.0019 Å
• b: 22.134 ± 0.002 Å
• c: 28.323 ± 0.003 Å
• α: 97.443 ± 0.005°
• β: 95.464 ± 0.005°
• γ: 107.43 ± 0.005°
• Cell volume: 10334.2 ± 1.9 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1215
• Residual factor for significantly intense reflections: 0.1051
• Weighted residual factors for significantly intense reflections: 0.2719
• Weighted residual factors for all reflections included in the refinement: 0.282
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No