Information card for entry 1529237

Structure parameters

• Chemical name: Catena-tetrakis(mu~3~-1,3-diethyl-2-thiobarbiturato-O,O',S)-dilead(II)
• Formula: C16 H22 N4 O4 Pb S2
• Calculated formula: C16 H22 N4 O4 Pb S2
• Title of publication: The crystal structure of lead(II) 1,3-diethyl-2-thiobarbiturate
• Authors of publication: Golovnev, Nikolay; Molokeev, Maxim; Golovneva, Irina
• Journal of publication: Russian Journal of Coordination Chemistry
• Year of publication: 2015
• Journal volume: 41
• Journal issue: 5
• Pages of publication: 300
• a: 12.9503 ± 0.0003 Å
• b: 12.9503 ± 0.0003 Å
• c: 32.0771 ± 0.001 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 4658.9 ± 0.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.0369
• Residual factor for significantly intense reflections: 0.0226
• Weighted residual factors for significantly intense reflections: 0.0381
• Weighted residual factors for all reflections included in the refinement: 0.0415
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes