Information card for entry 1529351

Structure parameters

• Formula: C4 H48 K0.28 N16 Ni2 O4 Rb7.72 Si18
• Calculated formula: C4 H48 K0.274 N16 Ni2 O4 Rb7.725 Si18
• Title of publication: The First Chelate-Free Crystal Structure of a Silicide Transition Metal Complex [K0.28Rb7.72Si9Ni(CO)2]2·16NH3
• Authors of publication: Gärtner, Stefanie; Hamberger, Markus; Korber, Nikolaus
• Journal of publication: Crystals
• Year of publication: 2015
• Journal volume: 5
• Journal issue: 3
• Pages of publication: 275
• a: 30.669 ± 0.006 Å
• b: 9.919 ± 0.002 Å
• c: 19.894 ± 0.004 Å
• α: 90°
• β: 110.18 ± 0.03°
• γ: 90°
• Cell volume: 5680 ± 2 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 8
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0568
• Residual factor for significantly intense reflections: 0.0349
• Weighted residual factors for significantly intense reflections: 0.0667
• Weighted residual factors for all reflections included in the refinement: 0.0711
• Goodness-of-fit parameter for all reflections included in the refinement: 0.954
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No