Information card for entry 1530387

Structure parameters

• Formula: C32 H59 N O4 Si2
• Calculated formula: C32 H59 N O4 Si2
• SMILES: [Si](CCCC(NC(=O)OCc1ccccc1)(C(=O)OC(C)(C)C)CCC[Si](CC)(CC)CC)(CC)(CC)CC
• Title of publication: Access to α,α-Disubstituted Disilylated Amino Acids and Their Use in Solid-Phase Peptide Synthesis.
• Authors of publication: Fanelli, Roberto; Salah, Khoubaib Ben Haj; Inguimbert, Nicolas; Didierjean, Claude; Martinez, Jean; Cavelier, Florine
• Journal of publication: Organic letters
• Year of publication: 2015
• Journal volume: 17
• Journal issue: 18
• Pages of publication: 4498 - 4501
• a: 16.472 ± 0.002 Å
• b: 18.563 ± 0.0004 Å
• c: 11.996 ± 0.002 Å
• α: 90°
• β: 92.581 ± 0.01°
• γ: 90°
• Cell volume: 3664.3 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.091
• Residual factor for significantly intense reflections: 0.0711
• Weighted residual factors for significantly intense reflections: 0.1853
• Weighted residual factors for all reflections included in the refinement: 0.2092
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No