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Information card for entry 1532475
Preview
Coordinates | 1532475.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C52 H67 Ge N Si |
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Calculated formula | C52 H67 Ge N Si |
SMILES | [Ge](N([Si](C(C)C)(C(C)C)C(C)C)c1c(cc(cc1C(c1ccccc1)c1ccccc1)C(C)C)C(c1ccccc1)c1ccccc1)C1CCCCCCC1 |
Title of publication | Two-coordinate group 14 element(ii) hydrides as reagents for the facile, and sometimes reversible, hydrogermylation/hydrostannylation of unactivated alkenes and alkynes |
Authors of publication | Hadlington, Terrance J.; Hermann, Markus; Frenking, Gernot; Jones, Cameron |
Journal of publication | Chem. Sci. |
Year of publication | 2015 |
Journal volume | 6 |
Journal issue | 12 |
Pages of publication | 7249 |
a | 9.942 ± 0.002 Å |
b | 15.413 ± 0.003 Å |
c | 28.793 ± 0.006 Å |
α | 90° |
β | 97.18 ± 0.03° |
γ | 90° |
Cell volume | 4377.5 ± 1.6 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0599 |
Residual factor for significantly intense reflections | 0.0501 |
Weighted residual factors for significantly intense reflections | 0.1404 |
Weighted residual factors for all reflections included in the refinement | 0.1476 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.037 |
Diffraction radiation wavelength | 0.7108 Å |
Diffraction radiation type | Synchrotron |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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