Information card for entry 1542498

Structure parameters

• Formula: C24 H33 N O Si
• Calculated formula: C24 H33 N O Si
• Title of publication: Gold vs Rhodium Catalysis: Tuning Reactivity through Catalyst Control in the C-H Alkynylation of Isoquinolones.
• Authors of publication: Shaikh, Aslam C.; Shinde, Dinesh R.; Patil, Nitin T.
• Journal of publication: Organic letters
• Year of publication: 2016
• Journal volume: 18
• Journal issue: 5
• Pages of publication: 1056
• a: 7.1879 ± 0.0012 Å
• b: 34.402 ± 0.006 Å
• c: 17.855 ± 0.003 Å
• α: 90°
• β: 91.042 ± 0.003°
• γ: 90°
• Cell volume: 4414.4 ± 1.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0977
• Residual factor for significantly intense reflections: 0.0746
• Weighted residual factors for significantly intense reflections: 0.2182
• Weighted residual factors for all reflections included in the refinement: 0.2429
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No