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Information card for entry 1542669
Preview
Coordinates | 1542669.cif |
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Original paper (by DOI) | HTML |
Formula | C26 H15 F3 S |
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Calculated formula | C26 H15 F3 S |
SMILES | c12ccccc1c1c(cccc1)C12c2ccccc2Sc2c1cc(cc2)C(F)(F)F |
Title of publication | Synthesis of Spirocyclic Diarylfluorenes by One-Pot Twofold SNAr Reactions of Diaryl Sulfones with Diarylmethanes. |
Authors of publication | Bhanuchandra, M.; Yorimitsu, Hideki; Osuka, Atsuhiro |
Journal of publication | Organic letters |
Year of publication | 2016 |
Journal volume | 18 |
Journal issue | 3 |
Pages of publication | 384 - 387 |
a | 7.4947 ± 0.0008 Å |
b | 10.4244 ± 0.0011 Å |
c | 12.3741 ± 0.0015 Å |
α | 83 ± 0.012° |
β | 82.694 ± 0.011° |
γ | 81.603 ± 0.007° |
Cell volume | 943.36 ± 0.19 Å3 |
Cell temperature | 93 ± 2 K |
Ambient diffraction temperature | 93 ± 2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.035 |
Residual factor for significantly intense reflections | 0.0331 |
Weighted residual factors for significantly intense reflections | 0.0909 |
Weighted residual factors for all reflections included in the refinement | 0.0922 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.075 |
Diffraction radiation wavelength | 1.54187 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/1542669.html
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