Information card for entry 1543103

Structure parameters

• Formula: C22 H41.5 N0.5 Na0.5 O Si U0.5
• Calculated formula: C22 H41.5 N0.5 Na0.5 O Si U0.5
• Title of publication: Steric control of redox events in organo-uranium chemistry: synthesis and characterisation of U(v) oxo and nitrido complexes
• Authors of publication: Tsoureas, Nikolaos; Kilpatrick, Alexander F. R.; Inman, Christopher J.; Cloke, F. Geoffrey N.
• Journal of publication: Chem. Sci.
• Year of publication: 2016
• Journal volume: 7
• Journal issue: 7
• Pages of publication: 4624
• a: 10.7251 ± 0.0002 Å
• b: 18.7626 ± 0.0003 Å
• c: 11.9516 ± 0.0002 Å
• α: 90°
• β: 95.238 ± 0.001°
• γ: 90°
• Cell volume: 2394.99 ± 0.07 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 11
• Hermann-Mauguin space group symbol: P 1 21/m 1
• Hall space group symbol: -P 2yb
• Residual factor for all reflections: 0.0343
• Residual factor for significantly intense reflections: 0.0305
• Weighted residual factors for significantly intense reflections: 0.0728
• Weighted residual factors for all reflections included in the refinement: 0.0762
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No