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Information card for entry 1543406
Preview
Coordinates | 1543406.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C17 H17 N |
---|---|
Calculated formula | C17 H17 N |
SMILES | [nH]1c2c(c3ccccc13)cc(c1c2C(C)CC1)C |
Title of publication | Carbazole Annulation via Cascade Nucleophilic Addition-Cyclization Involving 2-(Silyloxy)pentadienyl Cation. |
Authors of publication | Stepherson, Jacob R.; Ayala, Caitlan E.; Tugwell, Thomas H.; Henry, Jeffrey L.; Fronczek, Frank R.; Kartika, Rendy |
Journal of publication | Organic letters |
Year of publication | 2016 |
Journal volume | 18 |
Journal issue | 12 |
Pages of publication | 3002 - 3005 |
a | 15.4841 ± 0.0017 Å |
b | 20.8131 ± 0.0019 Å |
c | 7.9546 ± 0.0007 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 2563.5 ± 0.4 Å3 |
Cell temperature | 90 ± 0.5 K |
Ambient diffraction temperature | 90 ± 0.5 K |
Number of distinct elements | 3 |
Space group number | 45 |
Hermann-Mauguin space group symbol | I b a 2 |
Hall space group symbol | I 2 -2c |
Residual factor for all reflections | 0.034 |
Residual factor for significantly intense reflections | 0.0281 |
Weighted residual factors for significantly intense reflections | 0.071 |
Weighted residual factors for all reflections included in the refinement | 0.0722 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.041 |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/1543406.html
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Users of the data should acknowledge the original authors of the
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