Information card for entry 1544348

Structure parameters

• Formula: C11 H17 N O Si
• Calculated formula: C11 H17 N O Si
• SMILES: [Si](C)(C)(C)CNC(=O)c1ccccc1
• Title of publication: Site-Selective Silylation of Aliphatic C-H Bonds Mediated by [1,5]-Hydrogen Transfer: Synthesis of α-Sila Benzamides.
• Authors of publication: Liu, Pei; Tang, Jinghua; Zeng, Xiaoming
• Journal of publication: Organic letters
• Year of publication: 2016
• Journal volume: 18
• Journal issue: 21
• Pages of publication: 5536 - 5539
• a: 10.178 ± 0.004 Å
• b: 10.104 ± 0.004 Å
• c: 12.72 ± 0.005 Å
• α: 90°
• β: 108.216 ± 0.006°
• γ: 90°
• Cell volume: 1242.5 ± 0.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 7
• Hermann-Mauguin space group symbol: P 1 c 1
• Hall space group symbol: P -2yc
• Residual factor for all reflections: 0.1578
• Residual factor for significantly intense reflections: 0.133
• Weighted residual factors for significantly intense reflections: 0.3229
• Weighted residual factors for all reflections included in the refinement: 0.353
• Goodness-of-fit parameter for all reflections included in the refinement: 1.261
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No